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Zeamer Faraday Susceptometer

tech. notes on MAGNETIC MEASURING TECHNIQUES

Magnet's Faraday pole caps
Operator's view of cryostat and microbalance
MPMS Systems

   Cryostat (Model CTC-1)
    Low Temperature Gas/Liquid Supply System (LTSS)
   Bayonet Transfer Line
   10+ kilogauss Electromagnet
   Electromagnet Power Supply
   Microbalance
   Temperature Controller
   Rigid Structural Stand

Together this system can be used to detect superconductivity in 10 parts per million of a 10 mg sample. The system will detect proportionately smaller concentrations in samples of larger mass. This corresponds to a susceptibility sensitivity of 10-7 emu/g. The systems has a theoretical sensitivity of 10-6 emu/g.

The cryostat has a 0.585 inch inner diameter sample space. A low temperature gas/liquid supply system (LTSS) delivers the required cryogen to the cryostat through the vacuum insulated bayonet transfer line. Together the system controller and temperature controller can maintain temperatures to within 0.5K over a range from 4K to 800K. The temperature controller can interface with the optional system controller.

The microbalance has an accuracy of ±0.5 microgram with a repeatability of 0.2 microgram. The maximum balance capacity is 3.5 grams (1 00 grams optional). The microbalance can be interfaced with the optional system controller.

The electromagnet and power supply system is essential for precise magnetism experiments. The basic magnet is a horizontal field, variable gap electromagnet. The air gap is adjustable between 0" and 4.00" with an intercoil spacing of 4.00". Faraday pole pieces are provided to create a region of uniform force for susceptibility measurements. The power supply includes a water flow interlock to interrupt current to the magnet if cooling water flow stops. The electromagnet and power supply system can interlace with the optional system controller.

The stand's construction is welded steel for holding the Cryostat, Electromagnet, Instrument Support Module, and other system components.

Optional furnace (1100° C)
Computer controlled cryogenic delivery system

General Technical Specifications
Specifications may vary depending on final configuration
Differential Sensitivity 4x10-9 emu/g change in mass susceptibility for a 50 mg sample at maximum field strength of .9 Tesla (change in magnetic moment of 1.8x10-6 emu of moment), theoretical sensitivity of 1x10-10 emu/gram for a sample of 50 mg.
Measurement Range ± 0.05 emu of moment at full field level. Larger increments can be measured at lower field leveIs.
Sample Temperature Range: 4K to 800K
Stability: Dependent on temperature controller selected and cryogen supply settings
Rate of Change, Cooling: 300K to 77K in 5 minutes
Rate of Change, Heating: 300K to 800K in 30 minutes
Magnet/Power Supply
Performance
Field Range: ±l0 KGauss (±l Tesla); option ±1.5 Tesla
Field Gradient at sample position : 0 - 1800 gauss/cm, proportional to field
Region of Uniform H X dH/dx (uniform force): ± 1% over 5 mm DSV (0.1 cc volume)
Current Stability: 1 in 15 long-term
Current Resolution: 10-6 of full scale
Residual Field: 100 gauss
Microbalance System Sensitivity: 0.1 micrograms (10-4 dynes)
Maximum Load: 1.5 grams
Precision: 0.001% of load + 0.2 microgram
Cryostat (CTC-1) Vapor shielded, welded, stainless steel, continuous flow type sample cryostat
Gas surrounding sample (normally He) is independent of cryogen being used
Cryogen is only needed for sample temperatures below ambient, and either liquid N2, or He may be used
Abbess Instruments' LTSS and Bayonet Transfer Line
Computer Controller (Optional) Computer with, interfaces for reading balance output, and controlling magnet current and sample temperature
Open software for easier user modifications
The Instrument Support Module allows computer operational control of cryogen flow and sample gases
General Environmental Requirements 208-240 VAC, 60 Hz 3-phase, 3.8 KVA for magnet supply
110 VAC, 60 Hz, 15 amps for balance of electronics (optional 220 VAG, 50 Hz for all electronics)
Cooling water: 4 liters/min , 30 - 90 psi, no back pressure (closed loop chillers optional) for electromagnet
Floor space approximately 60 sq. ft. (.8 m 2); location of magnet power supply, computer console and LTSS is variable; no special coiling height requirement
Gross weight 850 lbs. (390 kg)

Faraday and Hall Measurement System Resistivity & Critical Control Option

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Thursday, April 09, 2009