Zeamer Faraday Susceptometer
tech. notes on MAGNETIC MEASURING TECHNIQUES
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Together this system can be used to detect superconductivity in 10 parts per million of a 10 mg sample. The system will detect proportionately smaller concentrations in samples of larger mass. This corresponds to a susceptibility sensitivity of 10-7 emu/g. The systems has a theoretical sensitivity of 10-6 emu/g. The cryostat has a 0.585 inch inner diameter sample space. A low temperature gas/liquid supply system (LTSS) delivers the required cryogen to the cryostat through the vacuum insulated bayonet transfer line. Together the system controller and temperature controller can maintain temperatures to within 0.5K over a range from 4K to 800K. The temperature controller can interface with the optional system controller. The microbalance has an accuracy of ±0.5 microgram with a repeatability of 0.2 microgram. The maximum balance capacity is 3.5 grams (1 00 grams optional). The microbalance can be interfaced with the optional system controller. The electromagnet and power supply system is essential for precise magnetism experiments. The basic magnet is a horizontal field, variable gap electromagnet. The air gap is adjustable between 0" and 4.00" with an intercoil spacing of 4.00". Faraday pole pieces are provided to create a region of uniform force for susceptibility measurements. The power supply includes a water flow interlock to interrupt current to the magnet if cooling water flow stops. The electromagnet and power supply system can interlace with the optional system controller. The stand's construction is welded steel for holding the Cryostat, Electromagnet, Instrument Support Module, and other system components. |
| General Technical Specifications Specifications may vary depending on final configuration |
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| Differential Sensitivity | 4x10-9 emu/g change in mass susceptibility for a 50 mg sample at maximum field strength of .9 Tesla (change in magnetic moment of 1.8x10-6 emu of moment), theoretical sensitivity of 1x10-10 emu/gram for a sample of 50 mg. |
| Measurement Range | ± 0.05 emu of moment at full field level. Larger increments can be measured at lower field leveIs. |
| Sample Temperature | Range: 4K to 800K Stability: Dependent on temperature controller selected and cryogen supply settings Rate of Change, Cooling: 300K to 77K in 5 minutes Rate of Change, Heating: 300K to 800K in 30 minutes |
| Magnet/Power Supply Performance |
Field Range: ±l0 KGauss (±l Tesla); option ±1.5 Tesla Field Gradient at sample position : 0 - 1800 gauss/cm, proportional to field Region of Uniform H X dH/dx (uniform force): ± 1% over 5 mm DSV (0.1 cc volume) Current Stability: 1 in 15 long-term Current Resolution: 10-6 of full scale Residual Field: 100 gauss |
| Microbalance System | Sensitivity: 0.1 micrograms (10-4 dynes) Maximum Load: 1.5 grams Precision: 0.001% of load + 0.2 microgram |
| Cryostat (CTC-1) | Vapor shielded, welded, stainless steel, continuous flow type sample cryostat Gas surrounding sample (normally He) is independent of cryogen being used Cryogen is only needed for sample temperatures below ambient, and either liquid N2, or He may be used Abbess Instruments' LTSS and Bayonet Transfer Line |
| Computer Controller (Optional) | Computer with, interfaces for reading balance output, and controlling magnet current and sample temperature Open software for easier user modifications The Instrument Support Module allows computer operational control of cryogen flow and sample gases |
| General Environmental Requirements | 208-240 VAC, 60 Hz 3-phase, 3.8 KVA for magnet supply 110 VAC, 60 Hz, 15 amps for balance of electronics (optional 220 VAG, 50 Hz for all electronics) Cooling water: 4 liters/min , 30 - 90 psi, no back pressure (closed loop chillers optional) for electromagnet Floor space approximately 60 sq. ft. (.8 m 2); location of magnet power supply, computer console and LTSS is variable; no special coiling height requirement Gross weight 850 lbs. (390 kg) |
Faraday and Hall Measurement System
Resistivity & Critical Control Option
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